Model 800 Viscometer Instruction Manual
Model 800 Viscometer Instruction Manual
Instruction Manual
Updated 5/5/2014
Ver. 2.15
Table of
Contents
Introduction.....................................................................................2
Description ......................................................................................2
Components....................................................................................3
Specifications..................................................................................5
Safety................................................................................................8
Setup.............................................................................................. 11
Calibration......................................................................................12
Operation.......................................................................................15
Calculations...................................................................................17
Disassembly..................................................................................17
Maintenance...................................................................................18
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Introduction
Description
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Components
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Optional:
#132-56-C R1 Closed-Cup Rotor; 316 Stainless Steel (For completion and
fracturing fluid testing.)
#130-45-1 Calibration Instrument
#132-58-7 Bob, B1, Threaded, Hollow, 303 Stainless Steel (Recommended for use with F0.2 spring)
#132-80
Calibration Fluid, Certified, 100 cP, 16 oz
Additional Bobs, Sleeves, and Springs:
#132-58-1 B2 Bob, 303 Stainless Steel
#132-58-2 B3 Bob, 303 Stainless Steel
#132-58-3 B4 Bob, 303 Stainless Steel
#132-58-4 B5 Bob, 303 Stainless Steel
#132-58H B1 Bob, Hastelloy
#132-56H
R1 Sleeve, Hastelloy
#134-10-2
#134-10-3
#134-10-4
#134-10-5
#134-10-6
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Specifications
Instrument Geometry
.1
Readout
Power Requirements
Weight (kg)
Dimensions (cm)
Shipping Weight (kg)
Shipping Dimensions (cm)
Direct Dial
13 - 16 VDC
6.0
15.2 17.8 40.6
20.4
55.9 25.4 40.6
R1B1
1.8415
1.7245
3.8
0.117
0.9365
R1B2
1.8415
1.2276
3.8
0.6139
0.666
R1B3
1.8415
0.8622
3.8
0.9793
0.468
R1B4
1.8415
0.8622
1.9
0.9793
0.468
R1B1
R1B2
R1B3
R1B4
F 0.2 (Green)
F 0.5 (Yellow)
F 1.0 (Blue)
F 2.0 (Red)
F 3.0 (Purple)
F 4.0(White)
F 5.0 (Black)
F 10.0 (Orange)
330
840
1680
3360
5040
6720
840
16800
651
1657
3314
6629
9943
13257
16571
33143
1320
3359
6717
13435
20152
26870
33587
67175
2644
6730
13460
26921
40381
53841
67302
134603
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R1B1
R1B2
R1B3
R1B4
1.7023
0.3770
0.2682
0.2682
5.11
1.13
0.80
0.80
10.21
51.07
102.14
170.23
340.46
510.69
1021.38
2.26
11.31
22.62
37.70
75.40
113.10
226.20
1.61
8.05
16.09
26.82
53.64
80.46
160.92
1.61
8.05
16.09
26.82
53.64
80.46
160.92
Viscosity Ranges<a>
(cP)
R1B1
R1B2
R1B3
R1B4
Minimum Viscosity<b>
@600 RPM
0.5<c>
4.5
12.7
25
Maximum Viscosity<d>
10,000,000 89,000,000 255,000,000 500,000,000
@0.01 RPM
<a> Computed for standard Torsion Spring (F 1.0). For other torsion 160.92springs, multiply by F factor
<b> Lower viscosities can be measured by the Model 900, however one must take into account the
effect of bearing drag, Taylor vortices, zero offset, etc. when looking at the expected accuracy of the
reading
<c> For practical purposes the minimum viscosity is limited to 0.5 cP due to Taylor Vortices
<d> Maximum viscosity is based on Maximum Shear Stress and Minimum shear rate (RPM). However,
due to practical and physical limitations, it may be difficult to take these measurements.
Viscosity Conversions
To convert from units on left side to units on top, multiply by factor @ intercept.
Centipoise
Poise (P) g/(cm*s) (mN*s)m2
(cP)
Centipoise
1
(cP)
Poise (P)
100
g/(cm*s)
100
1
(mN*s)m2
mPa*s
1
(lb*s)
478.93
100 ft2
mPa*s
(lb*s)
100 ft2
0.01
0.01
0.002088
1
1
0.01
0.01
100
100
0.01
0.01
100
100
1
1
100
100
1
1
0.2088
0.2088
0.002088
0.002088
4.789
4.789
478.93
478.93
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Viscosity Conversions
To convert from units on left side to units on top, multiply by factor @ intercept.
Dyne/cm2
Pa
lb/100ft2
lb/ft2
DR
Dyne/cm2
1
10
4.788
478.8
5.107
Pa
0.1
1
0.4788
47.88
0.5107
lb/100ft2
0.2084
2.084
1
100
1.065
lb/ft2
0.002084
0.02084
0.01
1
0.01065
DR
0.1957
1.957
0.939
93.9
1
To estimate which spring might be best, use the formula below to calculate a
Minimum Spring factor, where one establishes the maximum RPM the fluid
is going to be tested at, as well as what the expected Apparent Viscosity
of the fluid at that RPM. If the Factor comes out as .87, then an F 1.0 spring
should be used. If it comes out as .16, then an F 0.2 spring would be best.
To cover all ranges, it may be necessary to use more than one spring.
RPM(max) * AV(max)
Minimum Spring Factor (F) =
BOB(F)*90000
Bob (1)
R1B1
1
R1B2
8.9
R1B3
25.4
R1B4
50.7
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Safety
Explanation of Symbols
Caution:Risk of Danger - This symbol directs the operator to consult the
instruction manual for safety related warnings. (ISO-7000-0434)
Whenever this symbol is used on the equipment, the user must
consult the manual to determine the nature of the hazard and any actions which have to be taken.
Fuse: This is the internationally recognized symbol for a user-replaceable
fuse. This symbol will be followed by information required to guide the
user to choose the proper replacement fuse.
Direct Current (DC): This symbol indicates an input (or output) that is
direct current only. (IEC 60417-5013)
Note: This symbol will indicate important notes and helpful hints for the
operation of the equipment.
Polarity: This symbol indicates that the equipment receives positive voltage on the center pin of the connector and the return voltage is on the
outer case
Tip: This symbol is used to identify operational information and best practices to obtain the most reliable data.
Caution:Note - This symbol is used to indicate statements in the manual
which warn against actions which may cause damage to the equipment
during routine service or maintenance
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Electrical Requirements
The Model 800 Viscometer is to be powered by a DCpower source capable
of providing between 13 and 16 volts DC. The equipment is current limited
to 4 amps by a user-replaceable fuse. However, we suggest that the power
supply be current limited to less than 4 amps to provide additional protection
to the equipment.
Power (On/Off) Switch
Input Connector:
13 - 16 VDCPower
Inlet / Emergency
Disconnect Device
When connecting the equipment to your power source, make sure that the
13 - 16 VDC is connected to the center pin of the connector.
The equipment is supplied with a user-replaceable fuse. This fuse must only
be replaced by a 250-volt, 4-amp, time-delayed fuse.
Environmental Conditions
The equipment is designed for use in normal environmental conditions:
- Indoors
- At or below an altitude of 2,000 m (6,562 ft)
- In temperatures between 5 and 40C(41 - 104F)
- With a maximum relative humidity of 80% for temperatures up to
31C (88F) decreasing linearly to 50% relative humidity at 40C
(104F)
- This equipment has not been rated according to IEC 60529
Installation
The Model 800 Viscometer should be used in a location where it will not be
subjected to excessive moisture. It should be placed on a flat, stable surface in a well-ventilated environment.
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Caution - Risk of Danger: The samples presented for testing may contain
flammable substances. The following risk-reduction procedures must be followed to ensure the safe operation of the equipment.
-
-
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10
Setup
Rotor
Splash Guard
Bob
Sleeve
Platform
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Calibration
The Model 800 viscometer can lose calibration while in service if the bob
shaft bearings become contaminated or if the bob shaft itself is bent. If the
dial does not read zero when it should or if there is excessive dial deflection
when the main shaft is turning, this may indicate that the bob shaft bearings
are sticking. If the spring appears to be non-linear, the bob shaft may be
bent. Your viscometer will require servicing if it exhibits any of these symptoms.
According to API Recommended Practice 10B-2, viscometers being used
for testing well cement should be calibrated quarterly. API Recommended
Practice 13B-1 and 13B-2 specify viscometers being used for drilling fluids
should be checked monthly.
The OFITE Calibrating Instrument (Part No. 130-45-1) and the Calibration Check Kit (Part No. 132-49) are available to facilitate calibration. The
Calibrating Instrument uses a dead-weight method of calibrating, while the
Calibration Check Kit is fluid based. Both are provided in the Model 800
spare parts kit (Part No. 130-10-SP).
Equipment:
#130-45-1 Calibrating Instrument for 8-Speed Viscometer (Requires a
trained technician)
#132-49 Calibration Check Kit
Calibration Fluids, Certified:
#132-84 Calibration Fluid, 20 CP, 16 oz (500 mL)
#132-81 Calibration Fluid, 50 CP, 16 oz (500 mL)
#132-80 Calibration Fluid, 100 CP, 16 oz (500 mL)
#132-83 Calibration Fluid, 200 CP, 16 oz (500 mL)
#132-82 Calibration Fluid, 500 CP, 16 oz (500 mL)
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Procedure:
1. Choose the certified calibration fluid using the temperature-viscosity
chart supplied with the calibration fluid to cover the viscosity range of
interest. Make sure the lot number on the chart matches the lot number
on the fluid container. Each lot of standard fluid is individually certified.
The viscosity will normally vary slightly from lot to lot.
2. Clean and dry the viscometer bob, sleeve, and cup. Place the viscometer and the calibration fluid side-by-side on the counter top in a room
with a reasonably constant temperature (variation of less than 5F
2.5F). Allow the viscometer and the fluid to stand at least two hours to
equilibrate.
3. Operate the viscometer in air for two to four minutes to loosen up the
bearings and gears. Observe the rotor sleeve for excessive wobbling
and replace if necessary.
4. Fill the cup to the scribed line with calibration fluid and place it on the
viscometer stage. Move the stage upward until the fluid level is to the fill
line on the sleeve.
Never immerse the sleeve in fluids above the fill line.
Fill Line
Viscometer Sleeve
5. Place a thermometer capable of 0.2F (0.1C) into the fluid and hold
or tape it in place to prevent breakage. Operate the viscometer at a low
speed setting until the thermometer reading becomes stable to within
0.2F (0.1C) per 30 seconds. Note and record the temperature reading.
6. Once the temperature has stabilized, operate the viscometer at 600
RPM and then at 300 RPM. Note and record the dial readings to the
nearest 0.5 dial unit.
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Operation
Measuring Viscosity:
1. Mix the sample on the STIRsetting for 10 seconds while heating or
cooling the fluid. Monitor the temperature with a thermometer. Continue
to mix until the sample reaches the target temperature.
2. Rotate the knob to one of the speed settings. When the dial reading
stabilizes, record the reading and the temperature. Repeat this step for
any other speeds that your test requires.
Always start with the higher RPM and work your way down to the lowest
RPM. For example, if you need readings at 100 RPM, 200 RPM, and
300 RPM, record the measurement at 300 RPMfirst, then 200 RPM,
then 100 RPM, then gel strengths (if necessary).
When measuring gel properties, the dial does not have to return to zero
during the quiescent period. Therefore, it should not be forced back to
the zero setting if it does not freely do so. When determining the maximum dial deflection, no allowance needs to be made if the dial did not
start at zero. Only the maximum dial deflection is of interest. Rheological properties and characteristics of the sample will determine if the dial
returns to zero during the quiescent periods of the gel measurements.
4. For the 10 minute gel strength, re-stir the fluid and wait 10 minutes before recording the maximum dial deflection.
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APITesting
1. Mix the sample on the STIRsetting for 10 seconds.
2. Set the speed to 600 RPM. Wait for the reading to stabilize and then
record the dial reading and temperature.
3. Set the speed to 300 RPM. Wait for the reading to stabilize and then
record the dial reading and temperature.
4. Stir the sample again for 10 seconds.
5. Set the speed to GELand immediately shut off the power.
6. As soon as the sleeve stops rotating, wait 10 seconds and turn the
power on while looking at the dial. Record the maximum dial deflection
before the gel breaks. This is the 10 second gel strength.
7. For the 10 minute gel strength, re-stir the fluid and wait 10 minutes before recording the maximum dial deflection.
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Calculations
=K F
RPM
= Viscosity (cP)
Disassembly
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Maintenance
From time to time, the bearings will need to be changed. Complete the following to determine if it is time to perform this maintenance procedure:
1. The viscometer should have a zero dial reading when placed in an upright position with the sleeve not immersed in fluid prior to running tests.
2. With the instrument in this position, rotate the sleeve at 600 RPM. The
dial reading in air should not exceed one.
3. Place water in a suitable container and immerse the rotor sleeve to the
fill line.
4. Rotate the sleeve at 600 RPM. The dial reading in water should be between 1.5 and 3.0.
5. At 300 RPM, the dial reading in water should be between 0.5 and 2.0.
If the viscometer fails to pass any one of the above tests, the bearings are
bad and should be replaced by a qualified instrument technician.
Bob Shaft Bearing and Torsion Spring Replacement:
Tools Required:
Allen Wrench, 116"
Phillips Head Screwdriver
Retainer Ring Pliers (small)
External Retainer Ring Pliers
Flat Screw Driver
Bob Shaft Wrench
Replacement Parts:
#134-05-2
Bearing for Bob Shaft, Shielded
1. Unplug the power supply and remove the sleeve and bob.
Use the bob shaft wrench to hold the shaft in place while unscrewing the
bob.
2. With the flat-head screw driver, loosen the set screw in the speed control
knob. Remove the speed control knob from the unit.
3. Remove all four flat-head screws on the outer housing cover and gently
lift the cover upward.
4. Loosen the set screw at the top of the Zero Calibration Knob one turn
counterclockwise.
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5. Loosen the two screws in the top of the Index Block. Pull the Index
Block straight back to prevent damage to the dial or stop pin.
6. Loosen the top set screw on the dial one turn counterclockwise.
7. Gently lift the torsion spring straight up.
If you are replacing only the torsion spring, discard the old spring, and
skip to step 21 to complete the process.
Torsion Spring
Set Screw (Step 4)
Bridge
Dial
Bearing Mount
Index Block
8. Remove the four screws from the bridge, unclip the light, and lay the
bridge gently to the side.
9. While holding the bob shaft with the bob shaft wrench, loosen the set
screw (one turn counterclockwise) on the bottom of the dial. Remove the
bob shaft by pulling it straight down.
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10. Remove the two screws on the bearing mount and pull it straight up to
remove it.
Set Screw
Retainer Clip
Upper Bearing
Bearing Mount
Set Screw
11. The upper bearing is located inside the bearing mount. Use retaining
ring pliers to remove the retainer ring. Push the bearing upwards to
remove it from the bearing mount.
12. Use surgical gloves to insert a new upper bearing into the bearing
mount. Gently push downward to seat the bearing. Replace the retainer
ring with the retaining ring pliers.
Do not touch the bearing with bare hands. Dirt, oils, and other contaminants can damage the bearing.
13. Slide the bearing mount back onto the two pins and tighten the two
screws.
14. Remove the Splash Guard by sliding it straight down the shaft.
15. Loosen the set screw on the bearing shield (one turn counterclockwise).
Slide the bearing and bearing shield off the bob shaft.
16. Use surgical gloves to slide a new lower bearing onto the bob shaft.
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17. Slide the bearing shield back onto the bob shaft and tighten the set
screw. Slide the splash guard onto the bob shaft until in touches the
bearing shield.
Torsion Spring
Lower Bearing
Bearing Shield
Splash Guard
18. Slide the bob shaft up through the bearing mount. Turn the bob shaft
until the flat portion is facing the front of the unit.
19. Align the bottom set screw on the dial with the flat portion of the bob
shaft and tighten firmly. Make sure the set screws are perpendicular to
the top of the bob shaft.
20. Replace the bridge being careful not to touch or bend the encoder.
Tighten the four screws. Re-attach the light.
21. Gently slide the torsion spring through the Zero Calibration Knob and
into the dial. Make sure the bottom of the torsion spring is seated properly inside the dial. Tighten the set screw at the top of the dial to secure
the torsion spring.
22. Slide the index block into place. Tighten the two screws. Make sure the
zero mark on the dial is aligned with the mark on the index block.
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23. Press down on the torsion spring until the internal ring is flush with the
Zero Knob and tighten the set screw.
24. Loosen the set screw on the bridge on turn counterclockwise. Adjust the
Zero Calibration Knob so that the zero on the dial lines up with the line
on the index block. Tighten the set screw.
25. Replace the bob and sleeve.
26. Re-attach the main housing cover.
27. Re-attached the speed control knob.
28. Re-calibrate the instrument.
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