Asig 4-1
Asig 4-1
6:
Tratamientos Resultados
e -0.63
a 2.51
b -2.68
abe 1.66
c 2.06
ace 1.22
bce -2.09
abc 1.93
d 6.79
ade 5.47
bde 3.45
abd 5.68
cde 5.22
acd 4.38
bcd 4.30
abcde 4.05
a) Prepare a normal probability plot of the effects. Which effects seem active?
Normal Probability Plot of the Effects
(response is Results, Alpha = .05)
99
Effect Type
Not Significant
95 D Significant
90 F actor N ame
A A
80 B B
70 C C
Percent
60 D D
E E
50
40
30
20
10
5
1
-2 -1 0 1 2 3 4 5
Effect
Lenth's PSE = 0.76125
b) Calculate the residuals. Construct a normal probability plot of the residuals and plot the
residuals versus the fitted values. Comment on the plots.
0
50
10 -2
1
-4 -2 0 2 4 0.0 1.2 2.4 3.6 4.8
Re sidual F itte d V alue
2
Residual
1
-2
0
-3 -2 -1 0 1 2 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Re sidual O bse r v a tion O r de r
0
50
10 -2
1
-4 -2 0 2 4 0.0 1.2 2.4 3.6 4.8
Residual Fitted Value
2
Residual
1
-2
0
-3 -2 -1 0 1 2 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Residual Observation Order
Problema 8.8:
An article in Industrial and Engineering Chemistry uses a 25-2 design to investigate the effect of
A = condensation temperature, B = amount of material 1, C = solvent volume, D = condensation
time, and E = amount of material 2 on yield. The results obtained are as follows:
Tratamientos Resultados
e 23.2
ab 15.5
ad 16.9
bc 16.2
cd 23.8
ace 23.4
bde 16.8
abcde 18.1
a) Verify that the design generators used were I = ACE and I = BDE.
I + ACE + BDE
A + CE + BCD + ABDE
B + DE + ACD + ABCE
C + AE + ABD + BCDE
D + BE + ABC + ACDE
E + AC + BD + ABCDE
AB + CD + ADE + BCE
AD + BC + ABE + CDE
ABCD
A = CE = BCD = ABDE
B = DE = ACD = ABCE
C = AE = ABD = BCDE
D = BE = ABC = ACDE
E = AC = BD = ABCDE
AB = CD = ADE = BCE
AD = BC = ABE = CDE
ABCD
60 D D
E E
50
40
30
20
10
5
1
-7.5 -5.0 -2.5 0.0 2.5 5.0
Effect
Lenth's PSE = 2.7375
No se ve ningun factor significativo sin embargo se verifico que factor tiene un efecto mayor
sobre la respuesta con el siguiente grafico:
Main Effects Plot (data means) for Respuesta
A B C
22
20
Mean of Respuesta 18
16
-1 1 -1 1 -1 1
D E
22
20
18
16
-1 1 -1 1
d) Prepare an analysis of variance table. Verify that the AB and AD interactions are
available to use as error.
Alias Structure
I + A*C*E + B*D*E + A*B*C*D
A + C*E + B*C*D + A*B*D*E
B + D*E + A*C*D + A*B*C*E
C + A*E + A*B*D + B*C*D*E
D + B*E + A*B*C + A*C*D*E
E + A*C + B*D + A*B*C*D*E
A*D + B*C + A*B*E + C*D*E
A*B + C*D + A*D*E + B*C*E
Dejando las interacciones mencionadas por fuera no se obtiene aun grados de libertad para el
error. Sabiendo que B es el que mas impacta, se procedió a realizar una anova incluyendo solo el
factor B:
Factorial Fit: Respuesta versus B
Alias Structure
I
B
e) Plot the residuals versus the fitted values. Also construct a normal probability plot of the
residuals.
90
0.0
Residual
Percent
50
-2.5
10
1 -5.0
-5.0 -2.5 0.0 2.5 5.0 16 18 20 22
Residual Fitted Value
1.5 0.0
Frequency
Residual
1.0
-2.5
0.5
0.0 -5.0
-5 -4 -3 -2 -1 0 1 2 1 2 3 4 5 6 7 8
Residual Observation Order
Se observa un comportamiento aproximadamente normal, pero parece que a mayor valor en la
respuesta mayor varianza en los residuales.
Problema 13.9:
An experiment was performed to investigate the capability of a measurement system. Ten parts
were randomly selected, and two randomly selected operators measured each part three times.
The tests were made in random order, and the data below resulted.
1 50 49 50 50 48 51
2 52 52 51 51 51 51
3 53 50 50 54 52 51
4 49 51 50 48 50 51
5 48 49 48 48 49 48
6 52 50 50 52 50 50
7 51 51 51 51 50 50
8 52 50 49 53 48 50
9 50 51 50 51 48 49
10 47 46 49 46 47 48
99
95
90
80
70
Percent
60
50
40
30
20
10
5
0.1
-3 -2 -1 0 1 2 3
Residual
b) Find point estimates of the variance components using the analysis of variance method.
σ2 = MSE = 1.5
σ2τβ = (MSAB – MSE) / n = (0.6018 - 1.5) / 3 < 0, asumiendo σ2τβ = 0
σ2τ = (MSB – MSAB) / an = (11.0018 - 0.6018) / 2*3 = 1.733
σ2β = (MSA – MSAB) / bn < 0, asumiendo σ2τ = 0