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Determination of Chlorides
Determination of Chlorides
THEORETICAL BACKGROUND
INTERFERENCE
APPARATUS
REAGENTS
PROCEDURE
I. Sample Preparation:
Use a 100mL sample or a suitable portion diluted to 100mL. If the
sample is highly colored, add 3mL of Al(OH)3 suspension, mix, let
it settle down, and filter. If sulfide, sulfite, or thiosulfate is present,
add 1mL of H2O2 and stir for 1minute.
II. Titration:
Directly titrate samples in the pH range 7 to 10. Adjust sample pH
in the range 7 -10 with H2SO4 or NaOH if not in this range. For
adjustments, preferably use a pH meter with non-chloride-type
reference electrode.
Steps