Titration Level 3: Buenaventura Aims
Titration Level 3: Buenaventura Aims
level 3
buenaventura
Aims
In level 3, you'll analyse samples from a batch of hair product that is suspected to be fake. You'll perform titration
experiments to work out the level of ammonia in the samples.
In each activity you'll be able to collect points. At the end of the level you can restart to improve your skills.
Initially the pH of the solution quickly decreases as the strong acid is added to the solution of the weak base.
Then you used the pipette to transfer exactly 25.00 cm3 of ammonia solution into a beaker.
Next you rinsed the burette with some of the hydrochloric acid solution.
Then you filled the burette with the hydrochloric acid solution.
Finally the burette was filled below the tap by running out some solution.
pH meter 100 Points
First you used the pH probe to obtain a plot of pH against volume added from the burette.
From the data, you selected methyl orange and bromothymol blue as suitable indicators for the titration experiment.
Final reading
28.15 27.00 27.95 27.75
(cm3)
Initial reading
10.35 9.65 10.40 10.20
(cm3)
Mean titre
17.55
(cm3)
The results of the trial and 1st accurate titration were excluded from the average volume calculation.
You performed titration experiments on the ammonia solution from the hair product, using methyl orange as indicator.
You performed a trial titration first to get a rough idea of the amount of solution needed.
You then performed accurate titrations until your results were concordant and calculated the mean titre from your
concordant results.
Concentration of hair product = 3.52 mol dm-3 - this will be 50× the value above because it was diluted.
You correctly determined that the ammonia content in the hair product is above the accepted limit for use in cosmetic
products
Review
Things I did well on:
In this titration you used hydrochloric acid of known concentration. A technique referred to as “standardising the
solution” is often performed on acids prior to the titration to ensure an accurate concentration is known. Why?
According to sigmaaldrich.com, standardising the solution is also known as titer determination, these techniques are
used for titration and it is considered as one of the most important preconditions for reliable and transparent titration.
Titration results will be reliable and accurately if we work with proper standardising the solution.