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  • Acqmeth

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    antonio palazzo
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    This document summarizes the instrument control parameters for a gas chromatography mass spectrometry (GCMS) method. It includes settings for the GC oven temperature program, inlet, column, mass spectrometer acquisition parameters, and tune parameters. The method is for a 41.875 minute run using an Agilent 19091S-433UI column with temperature program starting at 35°C and ramping to 290°C at 8°C/min with a 10 minute hold.

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    acqmeth

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    This document summarizes the instrument control parameters for a gas chromatography mass spectrometry (GCMS) method. It includes settings for the GC oven temperature program, inlet, column, mass spectrometer acquisition parameters, and tune parameters. The method is for a 41.875 minute run using an Agilent 19091S-433UI column with temperature program starting at 35°C and ramping to 290°C at 8°C/min with a 10 minute hold.

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    © All Rights Reserved
    Download as TXT, PDF, TXT or read online from Scribd
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    Download as txt, pdf, or txt
    54 views6 pages

    Acqmeth

    Uploaded by

    antonio palazzo
    This document summarizes the instrument control parameters for a gas chromatography mass spectrometry (GCMS) method. It includes settings for the GC oven temperature program, inlet, column, mass spectrometer acquisition parameters, and tune parameters. The method is for a 41.875 minute run using an Agilent 19091S-433UI column with temperature program starting at 35°C and ramping to 290°C at 8°C/min with a 10 minute hold.

    Copyright:

    © All Rights Reserved
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    of 6

    INSTRUMENT CONTROL PARAMETERS: GCMS

    --------------------------------------

    C:\MassHunter\GCMS\1\METHODS\TDUBetteraveGazSaver2022.M
    Wed Feb 15 23:26:42 2023

    Control Information
    ------- -----------

    Sample Inlet : GC
    Injection Source : External Device
    Mass Spectrometer : Enabled

    Injection Location: Rear

    No Sample Prep method has been assigned to this method.

    GC
    GC Summary
    Run Time 41.875 min
    Post Run Time 0 min

    Oven
    Temperature
    Setpoint On
    (Initial) 35 °C
    Hold Time 0 min
    Post Run 50 °C
    Program
    #1 Rate 8 °C/min
    #1 Value 290 °C
    #1 Hold Time 10 min

    Equilibration Time 0.05 min


    Max Temperature 350 °C
    Maximum Temperature Override Disabled
    Slow Fan Disabled

    Front SS Inlet He
    Mode Pulsed Splitless
    Heater Off
    Pressure Off
    Total Flow Off
    Septum Purge Flow Off
    Septum Purge Flow Mode Standard
    Pre-Run Flow Test Off
    Injection Pulse Pressure 25 psi Until 0.5 min
    Purge Flow to Split Vent 100 mL/min at 1 min
    Liner Agilent 5190-2293: 900 μL (Splitless,
    single taper, wool, Ultra )

    Back PTV Inlet He


    Mode Solvent Vent
    Pressure On 6.7776 psi
    Total Flow On 54 mL/min
    Septum Purge Flow On 3 mL/min
    Septum Purge Flow Mode Standard
    Pre-Run Flow Test Off
    Gas Saver On 20 After 3 min mL/min
    Purge Flow to Split Vent 50 mL/min at 1.2 min
    Vent Flow 100 mL/min per min
    Vent Pressure 7.5 psi Until 0.05 min
    Liner Agilent 18740-80200: 140 μL (Direct,
    straight (gas samples, HS, P&)

    Column
    Column #1
    Flow
    Setpoint On
    (Initial) 1 mL/min
    Post Run 1 mL/min

    Column Information Agilent 19091S-433UI: 0684951H


    HP-5MS UI
    Temperature Range -60 °C—325 °C (350 °C)
    Dimensions 30 m x 250 μm x 0.25 μm
    Column lock Locked
    In Back PTV Inlet He
    Out MSD
    (Initial) 35 °C
    Pressure 6.7776 psi
    Flow 1 mL/min
    Average Velocity 36.169 cm/sec
    Holdup Time 1.3824 min
    Control Mode Constant Flow

    Column Outlet Pressure 0 psi

    Detector Evaluation
    Perform Detector Evaluation Test On
    Signal Selected No Signal Selected
    Checkout Sample NONE

    MSD Transfer Line


    Temperature
    Setpoint On
    (Initial) 250 °C

    Signals
    Signal #1:
    Description None

    Signal #2:
    Description None

    Signal #3:
    Description None

    Signal #4:
    Description None

    Signal #5:
    Description None

    Signal #6:
    Description None

    Signal #7:
    Description None

    Signal #8:
    Description None

    GERSTEL MAESTRO

    SYSTEM SETTINGS
    Maestro Runtime : 41.88 min
    GC Cool Down Time : 4.00 min
    Cryo Timeout : 20.00 min

    GERSTEL CIS

    CIS : used

    CRYO COOLING
    Cryo Cooling : used

    TEMPERATURE PROGRAM
    Heater Mode : Standard

    Liner Type : 013882-010-00 glass liner CIS4, baffled, non


    deactivated
    Liner Max Temperature : 400 'C

    Initial Temperature : -40 'C


    Equilibration Time : 0.05 min
    Initial Time : 0.20 min
    Ramp 1
    Rate : 12.00 'C/s
    End Temp : 280 'C
    Hold Time : 5.00 min
    Ramp 2
    Rate : 0.0 'C/s

    Low Split : not used

    GERSTEL TD3.5+

    TEMPERATURE PROGRAM
    Initial Temperature : 30 'C
    Delay Time : 0.50 min
    Initial Time : 20.20 min
    Ramp 1
    Rate 1 : 60.0 'C/min
    End Temp 1 : 280 'C
    Hold Time 1 : 10.00 min
    Ramp 2
    Rate 2 : 0.0 'C/min

    TD3.5+ SETTINGS
    Transfer Temp : 300 'C
    Transfer Temp Mode : Fixed
    Desorption Mode : Solvent Venting
    Vent Time : 20.00 min
    Sample Mode : Retain Tube - Standby Cooling
    Standby Temp : 50 'C

    TD3.5+ LIQUID OPTION


    Liquid Option : not used - use these parameters if it becomes 'used'
    Sample Tray : Rack 1,VT54/2-CVM
    Fixed Liquid Vial : used
    Liquid Vial : 1
    Inject into Micro vial : not used

    GERSTEL DHS

    DHS : not used - use these parameters if it becomes 'used'


    DHS Module : DHS

    INJECTION TUBE
    Tube Tray : TDUTray1,VT40t/Tube
    Sync. Vial/Tube Numbers : used

    PURGE TUBE
    Purge Tube : not used - use these parameters if it becomes 'used'
    Purge Tube Tray :
    Tube Number :

    INCUBATION SETTINGS
    Incubation Temperature : 30 'C
    Incubation Time : 5.00 min

    AGITATION SETTINGS
    Agitator On Time : 10 s
    Agitator Off Time : 1 s
    Agitator Speed : 500 rpm

    TRANSFER HEATER SETTINGS


    TEMP : 50 'C

    PURGE PHASE SETTINGS


    Volume : 0.0 mL
    TRAPPING PHASE SETTINGS
    Volume : 200.0 mL
    Flow : 20.0 mL/min
    Trap Temperature : 25 'C
    Incubation Temperature : 30 'C

    DRYING PHASE SETTINGS


    Volume : 50.0 mL
    Flow : 10.0 mL/min
    Trap Temperature : 25 'C

    MS Information
    -- -----------

    General Information
    ------- -----------

    Acquisition Mode : Scan


    Solvent Delay (minutes) : 0
    Tune file : C:\MassHunter\GCMS\1\5977\ATUNE.U
    EM Setting mode Gain : 1.000000

    Normal or Fast Scanning : Normal Scanning


    Trace Ion Detection : Off
    Run Time (if MS only) : 10 minutes

    [Scan Parameters]
    Start Time : 0
    Low Mass : 30
    High Mass : 400
    Threshold : 150
    A/D Samples: : 4

    [MSZones]

    MS Source : 230 C maximum 250 C


    MS Quad : 150 C maximum 200 C

    Timed Events
    ----- ------
    Number Events= 0

    END OF MS ACQUISITION PARAMETERS

    TUNE PARAMETERS for SN: US2104R033


    ---------------------------------

    Trace Ion Detection is OFF.

    34.593 : EMISSION
    70.007 : ENERGY
    25.536 : REPELLER
    79.473 : IONFOCUS
    25.226 : ENTRANCE_LENS
    991.027 : EMVOLTS
    1026.4 : Actual EMV
    1.00 : GAIN FACTOR
    2382.000 : AMUGAIN
    139.375 : AMUOFFSET
    2.000 : FILAMENT
    0.000 : DCPOLARITY
    11.861 : ENTLENSOFFSET
    0.000 : Ion_Body
    0.000 : EXTLENS
    -55.000 : MASSGAIN
    -21.000 : MASSOFFSET

    END OF TUNE PARAMETERS


    ----------------------

    END OF INSTRUMENT CONTROL PARAMETERS


    ------------------------------------

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