Lab Report Chem Exp 5
Lab Report Chem Exp 5
NUMBER OF EXPERIMENT: 5
PERMANGANATE
GROUP: A4AS120127
GROUP MEMBERS:
N NAME STUDENT
O NUMBER
1 ABDUL HAFIZ BIN ABD GHAFAR 2022699322
2 HAZIM BIN HAWARI 2022854202
2. Objectives
• Apparatus:
- Volumetric flask (250 mL)
- Pipette (20 mL)
- Graduated cylinder (10 mL)
- Conical flasks (250 mL)
- Beaker (50 mL)
- Burette
• Chemicals:
- Sodium thiosulphate (Na2S2O3)
- 0.025 M standard KMnO4 solution
- 2.0 M sulphuric acid
4. Procedure
1. The burette was washed with tap water followed by distilled water. Then, it was
rinsed with about 5-10 mL of KMnO4 solution. Through the burette tip, the second
rinsing was ran. The burette was then clamped to the retort stand.
2. The burette was filled with KMnO4. The tip of the burette was completely filled and
contained no air bubbles. The initial burette reading was then recorded to two
decimal places.
3. 4 g of Sodium thiosulphate was weighed accurately using weight paper on an
analytical balance. The mass of Na2S2O3 was then recorded.
4. With the aid of a filter funnel, the weighed sample was carefully transferred to a
250 mL volumetric flask. The funnel was rinsed with distilled water into the
volumetric flask. Using a graduated cylinder, 10 mL sulfuric acid was added into
the volumetric flask. Distilled water was then added until the calibration mark. The
flask was capped and shook to obtain a homogenous solution.
5. About 50 mL of Na2S2O3 solution was poured into a small beaker. A pipette was
washed with distilled water and rinsed with Na2S2O3 solution. Then, 20 mL of
Na2S2O3 solution was pipetted into a conical flask.
6. Using a graduated cylinder, 10 mL of sulphuric acid was added into the conical
flask.
7. The solution with the standard KMnO4 solution was titrated from the burette until
the end point is reached. The final burette reading was recorded to obtain the result
of the ROUGH TITRATION.
8. The titration process was then repeated until two consecutive titrations agree to ±
0.10mL.
5. Data Sheet
6. Calculations
3.318 𝑔
Concentration , g/L = 0.02 𝐿
= 165.9 g/L
7. Questions
Why did the solution turn to pink at the end of the titration?
8. Discussion
9. Conclusion