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ENVIROTEK LABORATORIES, INC.

120 White Owl Trail, Mullica Hill, NJ 08062 PHONE 856-478-0010 www.enviroteklab.com EPA ID # NJ01298 NJ DEP ID # 08012 PA DEP ID # 68-04402 NY ELAP # 11987 ADYA CLARITY VOC SPIKED SOLUTION TEST REPORT Report # 11-258-VOC Customer Name: Adya, Inc. Site Address: 445 East Chicago St. Coldwater, MI 49036 Report Date: November 3, 2011 EXECUTIVE SUMMARY A water solution prepared with a VOC standard concentration of 20 g/L of each organic volatile compound (VOC) was tested. Adya Clarity was added to separate beakers at a concentration of 1 mL and 2 mL of Adya Clarity per liter of VOC solution. The solutions were set in open beakers for 48 hours and tested after being filtered through the Adya Mineral Water Filter System. The concentration of VOCs were below the method detection limit for each compound on each solution. INTRODUCTION A water solution prepared with a VOC standard concentration 20 mg/L of each organic volatile compound (VOC) was tested. Adya Clarity was added to separate containers containing the VOC solution at a concentration of 1 mL of Adya Clarity and 2 mL of Adya Clarity per liter of VOC solution, respectively. The solutions were set in open containers for 48 hours; then tested after being filtered through the Adya Mineral Water Filter System. The concentration of VOCs were below the method detection limit for each compound on each solution. REAGENTS AND LAB EQUIPMENT HP 5890/5972 GC/MS system with ChemStation data system. Restek VMS GC column 60m, 0.25mm ID, 0.25um film. Restek VOC standard solution 2,000 mg/L solution. Adya Filter system. Adya Clarity solution. PROCEDURE A water solution was prepared using DI water and the Restek VOC standard solution to obtain a concentration of 20 ug/L of each VOC tested following the EPA method 524.2. One mL of Adya Clarity was added to one beaker containing one liter of the VOC solution, mixed well and let it stand for 48 hours in the open beaker. Two ml of Adya Clarity was added to a second beaker containing one liter of the VOC solution, mixed well and let it stand for 48 hours in the open beaker. The solutions were filtered through the Adya Mineral Water Filter System, the final filtered solutions were tested again for VOCs. One beaker containing one liter of the VOC solution was set parallel to the other solutions and let it stand for 48 hours for a control sample without adding any Adya Clarity and filtered through the Adya Mineral Water Filter System. The results are summarized in the table below.

CONFIDENTIAL Page 1 of 3

ENVIROTEK LABORATORIES, INC.


120 White Owl Trail, Mullica Hill, NJ 08062 PHONE 856-478-0010 www.enviroteklab.com EPA ID # NJ01298 NJ DEP ID # 08012 PA DEP ID # 68-04402 NY ELAP # 11987 RESULTS The VOC concentrations are summarized in the following table:
Test Parameter 20 ppb VOC Solution 19.24 ug/L 19.90 ug/L 17.58 ug/L 19.10 ug/L 18.65 ug/L 18.24 ug/L 18.25 ug/L 19.35 ug/L 18.84 ug/L 19.89 ug/L 18.71 ug/L 17.52 ug/L 18.88 ug/L 18.82 ug/L 19.15 ug/L 19.57 ug/L 19.33 ug/L 19.25 ug/L 18.71 ug/L 19.16 ug/L 19.88 ug/L 19.18 ug/L 19.55 ug/L 19.18 ug/L 18.94 ug/L 19.22 ug/L 19.73 ug/L 19.47 ug/L 19.18 ug/L 18.63 ug/L 19.45 ug/L 19.50 ug/L 18.32 ug/L 19.26 ug/L 19.20 ug/L 18.19 ug/L 18.40 ug/L 19.25 ug/L 19.10 ug/L 19.07 ug/L 19.65 ug/L 19.91 ug/L 19.28 ug/L 19.75 ug/L 19.75 ug/L 19.70 ug/L 18.08 ug/L 19.80 ug/L 18.36 ug/L 19.36 ug/L 19.20 ug/L 19.00 ug/L 19.05 ug/L 19.20 ug/L 18.60 ug/L 19.04 ug/L Control Filtered Solution (after 48 hrs) 2.35 ug/L 1.25 ug/L 1.85 ug/L 1.55 ug/L 1.85 ug/L 1.51 ug/L 3.52 ug/L 3.38 ug/L 2.35 ug/L 1.62 ug/L 1.35 ug/L 2.25 ug/L 1.52 ug/L 1.55 ug/L 1.52 ug/L 1.85 ug/L 1.35 ug/L 1.65 ug/L 1.75 ug/L 1.95 ug/L 0.72 ug/L 1.49 ug/L 0.58 ug/L 0.58 ug/L 2.18 ug/L 0.85 ug/L 1.45 ug/L 1.47 ug/L 0.58 ug/L 0.96ug/L 1.50 ug/L <0.5 ug/L 0.52 ug/L 0.53 ug/L 0.85 ug/L 0.55 ug/L 0.86 ug/L 0.76 ug/L 0.80 ug/L 0.65 ug/L 0.58 ug/L 1.25 ug/L 0.84 ug/L 0.68 ug/L <0.5 ug/L 0.60 ug/L <0.5 ug/L 0.53 ug/L 0.74 ug/L 0.66 ug/L 0.60 ug/L 0.20 ug/L 0.59 ug/L 0.95 ug/L <0.5 ug/L <0.5 ug/L 1 mL Adya Clarity Filtered Solution (after 48 hrs) <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L 2 mL Adya Clarity Filtered Solution (after 48 hrs) <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L

Acetone Acrylonitrile Allyl chloride Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chloroacetonitrile Chlorobenzene 1-Chlorobutane Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene 1,1-Dichloropropanone cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diethyl ether Ethylbenzene Ethyl methacrylate Hexachlorobutadiene Hexachlorobutadiene Hexachloroethane 2-Hexanone Isopropylbenzene 4-Isopropyltoluene Methacrylonitrile Methylacrylate Methylene chloride

CONFIDENTIAL Page 2 of 3

ENVIROTEK LABORATORIES, INC.


120 White Owl Trail, Mullica Hill, NJ 08062 PHONE 856-478-0010 www.enviroteklab.com EPA ID # NJ01298 NJ DEP ID # 08012 PA DEP ID # 68-04402 NY ELAP # 11987
Test Parameter 20 ppb VOC Fresh Solution 18.72 ug/L 18.87 ug/L 18.68 ug/L 18.57 ug/L 19.24 ug/L 19.85 ug/L 19.83 ug/L 18.70 ug/L 19.95 ug/L 19.15 ug/L 18.90 ug/L 19.55 ug/L 19.73 ug/L 18.66 ug/L 19.15 ug/L 18.57 ug/L 18.80 ug/L 18.54 ug/L 19.50 ug/L 19.95 ug/L 19.33 ug/L 19.50 ug/L 19.65 ug/L 19.85 ug/L 19.22 ug/L 19.50 ug/L 19.73 ug/L 19.11 ug/L 19.90 ug/L Control Solution (after 48 hrs) 0.85 ug/L <0.5 ug/L 0.61 ug/L 0.85 ug/L 1.35 ug/L 1.50 ug/L 0.68 ug/L 0.49 ug/L 0.60 ug/L 1.20 ug/L 1.22 ug/L 0.55 ug/L 1.42 ug/L 1.35 ug/L 0.72 ug/L 0.88 ug/L 1.44 ug/L 0.63 ug/L 0.68 ug/L 0.51 ug/L 1.44 ug/L <0.5 ug/L 1.35 ug/L 1.49 ug/L 3.50 ug/L <0.5 ug/L 1.87 ug/L 1.08 ug/L 1.38 ug/L 1 mL Adya Clarity Filtered Solution (after 48 hrs) <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L 2 mL Adya Clarity Filtered Solution (after 48 hrs) <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L <0.5 ug/L

Methyl iodide Methylmethacrylate 4-Methyl-2-pentanone Methyl-t-butyl ether Naphthalene Nitrobenzene 2-Nitropropane Pentachloroethane Propionitrile n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene m-Xylene p-Xylene

CONCLUSION The Adya Clarity is very effective when used to filter the volatile organic compounds through the Adya Mineral Water Filtration System.
Jaime A. Young Lab Director

CONFIDENTIAL Page 3 of 3

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